Multivariate Optimization of Supercritical Fluid Derivatization and Extraction of Phenol in Soil Samples
نویسندگان
چکیده
منابع مشابه
Response surface methodology for optimization of supercritical fluid extraction of orange peel essential oil
Background: Orange peel essential oils were obtained using supercritical fluid extraction. This method is an important high scaling extraction methods that used for extraction of plant and animal extracts. Methodology: The experimental parameters of SFE such as temperature, pressure, and extraction time and modifier volume were optimized using a central composite design after a 24-1fractional ...
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The research objective was to build a fully-continuous lab-scale supercritical fluid extraction process to remove naphthalene from soil slurries. Both the carbon dioxide and the soil slurry were pumped into an extraction vessel simultaneously and continuously for the duration of an experimental run. Delhi Loamy Sand spiked with approximately 10 000 ppm (wt) of naphthalene and water comprised th...
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high pressures also requires special equipment. In summary, both RESS crystallization and SAS crystallization appear to be promising methods for generating supersaturation and therefore represent alternatives to conventional crystallization. Such alternatives may prove attractive in applications such as polymer and pharmaceutical processing, or in particle design for drug delivery. It is possib...
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Optimizing the extracted analyte collection step in analytical supercritical fluid extraction (SFE) is of key importance in achieving high analyte recoveries and extraction efficiencies. Whereas the extraction step in SFE has been well characterized both theoretically and experimentally; the analyte collection step after SFE has few theoretical guidelines, aside from a few empirical studies whi...
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ژورنال
عنوان ژورنال: Journal of Chromatographic Science
سال: 1996
ISSN: 0021-9665,1945-239X
DOI: 10.1093/chromsci/34.1.43